Table 3 Crystallographic data for N-(pyridin-2-yl)hydrazinecarbothioamide

Formula

C₆H₈N₄S

Formula weight

168.22

Temperature/K

293

Crystal system

Monoclinic

Space group

C2/c

Lattice parameters

a/Å

15.5906 (7)

b/Å

10.1719 (5)

c/Å

11.1763 (6)

α/°

90.00

β/°

121.116 (3)

γ/°

90.00

V/ų

1517.39 (13)

Z

8

D_calc/g/cm³

1.473

F ₀₀₀

704

μ_Mo-Kα Å

0.71073

Reflections collected

7055

Independent reflections

2200

Data/parameters/restrains

2200/100/0

Goodness of fit on F²

1.041

Absorption coefficient mm⁻¹

0.36

Final R indices (I > 2.00σ(I))

R₁ = 0.0602, wR₂ = 0.1649

R indices (all data)

R₁ = 0.1385, wR₂ = 0.1965

Maximum/minimum residual electron density (e. Å⁻³)

0.397/− 0.489