Table 1 1 H- and13 C-NMR data of metabolite 4 in CDCl 3
Position | 4 | ||
|---|---|---|---|
δH (mult., Jin Hz)# | δ C ¤ | Mult. | |
1 | 4.53 brs | 70.1 | CH |
2 | 2.23 m, 1.65 m | 48.0 | CH2 |
3 | - | 218.2 | C |
4 | - | 46.8 | C |
5 | 1.35 m | 58.0 | CH |
6 | 1.71 m, 1.51 m | 34.1 | CH2 |
7 | 1.75 m, 1.48 m | 41.1 | CH2 |
8 | - | 79.2 | C |
9 | 1.42 m | 60.3 | CH |
10 | - | 35.7 | C |
11 | 1.69 m, 1.51 m | 22.9 | CH2 |
12 | 3.96 dt (3.3, 9.0), 3.81 dd (8.1, 16.5) | 64.4 | CH2 |
13 | 1.36 s | 21.9 | CH3 |
14 | 1.39 s | 14.9 | CH3 |
15 | 1.17 s | 24.7 | CH3 |
16 | 1.41 s | 23.4 | CH3 |