Fig. 1From: Freeze-drying: an alternative method for the analysis of volatile organic compounds in the headspace of urine samples using solid phase micro-extraction coupled to gas chromatography - mass spectrometryIntensity of compounds present in the reference solution throughout the experiment. A stock of reference solution was prepared at the beginning of the experiment. A 2 ml sample of the reference solution was analysed on the same days that urine samples were processed. The intensities of reference compounds were normalized by their intensities detected on day 1Back to article page