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Table 1 Percentage composition of the hexane extract from aerial parts of three Cistus spp

From: Antiproliferative activity of hexane extract from Tunisian Cistus libanotis, Cistus monspeliensis and Cistus villosus

Component

Ki

% CL

% CM

% CV

Hydrocarbons

 

9.3

22.8

37.3

Tricosane

2300

 

t

0.1

Pentacosane

2500

2.4

1.8

3.1

Heptacosane

2700

2.2

6.1

6.6

Octacosane

2800

0.3

3.6

t

Nonacosane

2900

3.3

7.1

18.3

Hentriacontane

3100

1.1

4.2

9.2

Carbonylic compounds

  

0.7

2.2

Undecan-2-one

1287

 

0.7

2.2

Monoterpene hydrocarbons

 

10.5

2.1

0.9

Tricyclene

928

0.1

  

α-Thujene

931

0.1

  

α-Pinene

938

2.1

  

Camphene

953

3.6

  

Sabinene

973

1.2

  

β-Pinene

980

3.0

  

α-Terpinene

1012

0.3

  

p-Cymene

1025

0.1

0.8

0.3

Limonene

1030

 

1.3

0.6

Sesquiterpene hydrocarbons

 

1.5

t

 

Cyclosativene

1363

t

  

α-Copaene

1377

t

  

α-Elemene

1398

0.2

  

β-Caryophyllene

1414

0.7

  

Widdrene

1433

 

t

 

γ-Elemene

1438

t

  

α-Humulene

1455

0.1

  

allo-Aromadendrene

1463

0.4

  

1-S-cis-Calamenene

1520

0.1

  

Oxygenated monoterpenes

 

6.6

2.0

1.1

1,8-Cineole

1034

0.1

1.1

0.4

cis-Sabinene hydrate

1063

t

  

trans-Sabinene hydrate

1086

0.7

  

α-Campholenal

1128

t

  

Camphor

1145

0.7

  

Borneol

1167

1.2

  

Myrtenol

1197

0.3

  

Linalyl acetate

1277

0.7

0.9

0.7

Isobornyl acetate

1284

0.3

  

Bornylacetate

1286

1.8

  

α-Terpenyl acetate

1343

0.8

  

Oxygenated sesquiterpenes

 

0.7

1.4

1.2

Globulol

1587

t

  

Viridiflorol

1593

0.4

1.4

1.2

Caryophylla-4(12),8(13)-dien-5β-ol; Caryophylladienol I

1640

0.2

  

Caryophylla-3,8(13)-dien-5-β-ol

1649

0.1

  

Diterpenes

 

2.2

3.8

4.8

Neophytadiene

1838

2.2

1.2

3.8

Cembrene

1943

 

t

 

Manoyloxide

1989

 

2.5

 

13-epi-Manoyl oxide

1994

  

0.8

(E)-Phytol

2132

 

t

0.2

2-keto-manoyl oxide

2210

 

t

 

3β-hydroxy- 13-epi- manoyl oxide

2273

 

0.1

 

Fatty acids and derivatives

 

24.4

43.3

10.6

Cinnamic acid

1397

  

0.2

Dodecanoic acid

1566

t

  

Tetradecanoic acid

1768

0.2

1.4

0.7

Pentadecanoic acid

1863

 

t

 

Phthalic acid, diisobutyl ester

1871

0.1

1.4

4.6

(Z,Z,Z)-9,12-15-Octadecatrienoic acid

2099

23.5

14.7

1.7

(Z,Z)-9,12-Octadecadienoic acid

2122

0.6

6.6

1.4

Octadecanoic acid

2172

 

0.5

0.1

Eicosanoic acid

2327

 

2.0

0.5

Docosanoic acid

2526

 

2.7

 

Tricosanoic acid

2628

 

0.4

 

Tetracosanoic acid

2730

 

6.3

1.4

Pentacosanoic acid

2829

 

2.2

 

Hexacosanoic acid

2934

 

4.3

 

Heptacosanoic acid

3032

 

0.8

 

Phenolic compounds

 

1.4

1.0

1.2

Carvacrol

1299

0.3

1.0

1.2

2,5-di-tert-butylphenol

1513

0.5

  

BHT

1515

0.6

  
 

R t

   

Flavonoids

 

30.2

0

0.1

Apigenin dimethyl ether (Genkwanin 4'-methyl ether)

43.26

5.6

  

Quercetagetin 3',4',6,7-tetramethyl ether

43.36

24.6

 

0.1

Quercetin 3,7,3',4'-tetramethyl ether (Retusin)

47.18

   

Others

 

3.3

16.2

32.8

Dihydroctinidiolide

19.26

 

0.2

0.7

Vitamin E

47.65

3.3

11.5

22.7

γ-Sitosterol

51.50

  

0.4

β-Amyrine

52.14

 

0.9

t

α-Amyrine

53.16

 

1.2

1.3

3β-Acetyloxyolean-12-en-28-oic acid methyl ester (Oleanolic acid methyl ester acetate)

65.18

  

0.5

Total amount of compounds

 

90.1

92.6

92.2

  1. Ki : linear retention indices; Rt: retention times; t: traces, less than 0.05%; CL: Cistus libanotis; CM: Cistus monspeliensis; CV: Cistus villosus.