Table 2 Selected bond lengths (Å), bond angles (°), and torsion angles (°)
C1-O1 | 1.369(2) | C4-Cl1 | 1.744(2) |
C2-C9 | 1.502(2) | C7-O1 | 1.423(2) |
C7-C8 | 1.523(2) | C8-O2 | 1.237(2) |
C8-O3 | 1.249(2) | C10-O4 | 1.420(2) |
C11-O4 | 1.419(2) | C12-O5 | 1.425(2) |
C13-O5 | 1.405(2) | C14-N1 | 1.490(2) |
C15-N1 | 1.500(2) | Â | Â |
O1-C1-C6 | 124.33(15) | O1-C1-C2 | 115.40(13) |
O1-C7-C8 | 115.00(14) | O2-C8-O3 | 126.33(16) |
O2-C8-C7 | 119.17(14) | O3-C8-O7 | 114.48(15) |
O4-C10-C15i | 109.71(13) | O4-C11-C12 | 108.92(15) |
O5-C12-C11 | 108.47(15) | O5-C13-C14 | 107.27(14) |
N1-C14-C13 | 110.33(14) | N1-C15-C10i | 113.09(14) |
C14-N1-C15 | 115.90(13) | C1-O1-C7 | 117.34(12) |
C11-O4-C1 | 112.78(13) | C13-O5-C12 | 111.91(13) |
O1-C1-C2-C3 | -178.46(15) | O1-C1-C2-C9 | -1.0(3) |
C2-C3-C4-Cl1 | -177.68(14) | O1-C7-C8-O2 | -15.4(2) |
O1-C7-C8-O3 | 166.31(14) | O4-C11-C12-O5 | 67.19(19) |
O5-C13-C14-N1 | -173.03(15) | C13-C14-N1-C15 | -179.80(15) |
C10i-C15-N1-C14 | -72.10(19) | C6-C1-O1-C7 | 5.5(2) |
C2-C1-O1-C7 | -174.16(16) | C8-C7-O1-C1 | -79.74(19) |
C12-C11-O4-C10 | -167.40(15) | C15i-C10-O4-C11 | 167.28(14) |
C14-C13-O5-C12 | -175.94(15) | C11-C12-O5-C13 | 179.36(16) |